Hydrochloric Acid → N-Methyl-N(4-t-Butylphenylthiosulfenyl) Carbamoyl Fluoride
反応式
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([SH:11])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].CN(Cl)C(F)=S.Cl.[CH3:19][N:20]([S:24]SC1C=CC(Cl)=CC=1)[C:21]([F:23])=[O:22]>CCCCC>[CH3:19][N:20]([S:24][S:11][C:8]1[CH:7]=[CH:6][C:5]([C:1]([CH3:4])([CH3:2])[CH3:3])=[CH:10][CH:9]=1)[C:21]([F:23])=[O:22]参加物
6
実験手順
Prepared by reacting 0.5 g of 4-t-butylthiophenol in pentane with 0.44 g of N-methyl-N-chlorothiocarbamoyl fluoride. The reaction proceded with a vigorous exotherm and evolution of hydrochloric acid gas. The infrared and n.m.r. spectra of the product was identical to the material prepared by Method I.
後処理
- customPrepared
出典と根拠
- ORDレコード
- ord-fa71a60d6f244171a56e63b8bc36ee36
- 出典データセット
- uspto-grants-1978_05
- 特許番号
- US04091016
反応ノート
読み込み中…