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Hydrochloric Acid → Glycyl-glycine benzyl ester hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Benzyl (tert-butoxycarbonyl)glycylglycinate | HCID 3244524 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | Glycyl-glycine benzyl ester hydrochloride | HCID 13996146 | — |
反応手順
10.3 Parts N-t-butoxycarbonylglycylglycine benzyl ester is dissolved in 200 parts dioxane and treated with a 10 fold excess of 2 N hydrochloric acid in dioxane for 10 minutes. Removal of the solvent under reduced pressure affords pure glycylglycine benzyl ester hydrochloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04092304 |
| 出典データセット | uspto-grants-1978_05 |
| ORD ID | ord-649622d36011435d853bf41132b09046 |
| 出典メモ | uspto-grants-1978_05 |