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2-Ethylaniline → 2,2'-Dithiobis[N-(2-ethylphenyl)benzamide]
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Ethylaniline | HCID 11357 | — |
| 反応物 | 2,2'-Dithiodibenzoyl chloride | HCID 88164 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 2,2'-Dithiobis[N-(2-ethylphenyl)benzamide] | HCID 18935325 | 33.6% |
反応手順
This compound was prepared according to the general method of Example 90 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 2-ethylaniline (1.40 g, 11.6 mmol) in 12 mL of pyridine. The crude product was recrystallized from acetonitrile-DMF to yield 1.0 g of the title compound, mp 255°-256° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05734081 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-7d989fed42294e84a3366f42f847f891 |
| 出典メモ | uspto-grants-1998_03 |