関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | Heptanenitrile, 7-bromo- | HCID 88737 | — |
| 反応物 | 2,2'-[iminobis(ethane-2,1-diyl)]bis(1H-isoindole-1,3(2H)-dione) | HCID 354707 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | (6-Cyanohexyl)bis(2-phthalimidoethyl)amine | HCID 19811078 | — |
反応手順
A mixture of 6-bromohexylcyanide (1) (13.88 g, 0.073 mol), bis(2-phthalimidoethyl)amine (2) (26.52 g, 0.073 mol), and triethylamine (7.37 g, 0.073 mol) in DMF (120 ml) was heated at 100° C. for 20 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05162109 |
|---|
| 出典データセット | uspto-grants-1992_11 |
|---|
| ORD ID | ord-686a09d02c0048e0845c63a7c6ad7214 |
|---|
| 出典メモ | uspto-grants-1992_11 |
|---|
