化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → Acryloylglycine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Sodium Pyrrolidone Carboxylate | HCID 23666346 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Acryloylglycine | HCID 100321 | 234.1% |
反応手順
100 g of 25 wt % polyacrylic acid aqueous solution (viscosity 8000-12000 cps, 30 ° C.) and 3 g of N-carboxy methyl acrylamide were polymerized at 70° C. for 3 hours for partial crosslinking. Sodium hydroxide was added to neutralize the pH value to 7.0 and 20 g of poly(ether alcohol)(GEP-2800, Dow Chemical Co., U.S.A.) and 1.5 g of sodium 2-pyrrolidone-5-carboxylate were added. Deionized water was then added to the resulting product to adjust the solid content thereof to 35 wt %. The viscosity of the resultant solution was measured as 6000 to 6500 cps(30° C.). The resulting product was tested according to the procedures as set forth in Example 1 and the test results are listed in Table 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05420182 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-fdac4201e63c4de3ae7bc8303e691d9b |
| 出典メモ | uspto-grants-1995_05 |