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HRID 37315作成日:2026年10月26日

Propylene Oxide → Acryloylglycine

https://huagongshe.com/reaction/37315

反応式

関与物質

役割名称HCID仕込み量
反応物Propylene OxideHCID 6378—
反応物Potassium HydroxideHCID 14797—
反応物Sodium Pyrrolidone CarboxylateHCID 23666346—
溶媒WaterHCID 962—
生成物AcryloylglycineHCID 100321292.6%

反応手順

100 g of 25 wt % polyacrylic acid aqueous solution and 2.5 g of N-carboxy methyl acrylamide were polymerized at 60° C. for 3 hours for partial crosslinking. Potassium hydroxide was added to neutralize the pH value to 7.0 and 40 g of T-P400(polymer of triol and propylene oxide, Union Carbide Co., U.S.A.) and 1 g of sodium 2-pyrrolidone-5-carboxylate were added. Deionized water was then added to the resultant product to adjust the solid content thereof to 35 wt %. The viscosity of the resultant solution was measured as 5500 to 6000 cps(30° C.). The resulting product was tested according to the procedures set forth in Example 1, and the test results are listed in Table 1.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05420182
出典データセットuspto-grants-1995_05
ORD IDord-6090913c96ce484f959002b7770a8a83
出典メモuspto-grants-1995_05