化工社化工社 化学情報印刷レポート · 研究参考用
Propylene Oxide → Acryloylglycine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Propylene Oxide | HCID 6378 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | Sodium Pyrrolidone Carboxylate | HCID 23666346 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Acryloylglycine | HCID 100321 | 292.6% |
反応手順
100 g of 25 wt % polyacrylic acid aqueous solution and 2.5 g of N-carboxy methyl acrylamide were polymerized at 60° C. for 3 hours for partial crosslinking. Potassium hydroxide was added to neutralize the pH value to 7.0 and 40 g of T-P400(polymer of triol and propylene oxide, Union Carbide Co., U.S.A.) and 1 g of sodium 2-pyrrolidone-5-carboxylate were added. Deionized water was then added to the resultant product to adjust the solid content thereof to 35 wt %. The viscosity of the resultant solution was measured as 5500 to 6000 cps(30° C.). The resulting product was tested according to the procedures set forth in Example 1, and the test results are listed in Table 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05420182 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-6090913c96ce484f959002b7770a8a83 |
| 出典メモ | uspto-grants-1995_05 |