関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Citric Acid | HCID 311 | — |
| 反応物 | Glyoxylylspermidine | HCID 133564 | — |
| 反応物 | HCID 178479429 | HCID 178479429 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178512808 | HCID 178512808 | — |
反応手順
A mixture of 10.0 g (45.0 m moles) of 7-guanidinoheptanamide hydrochloride, 13.1 g (45.0 moles) of N-[4-(3-aminopropyl)aminobutyl]-2,2-dihydroxyethanamide dihydrochloride, and 3.2 g (15 m moles) of citric acid in water (100 ml) was evaporated to dryness to give a syrup which contained 1.0 g of water. The resulting syrup was heated at 60° C. for 8 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05162581 |
|---|
| 出典データセット | uspto-grants-1992_11 |
|---|
| ORD ID | ord-cab24a28696d4348b9815b96e24e4dba |
|---|
| 出典メモ | uspto-grants-1992_11 |
|---|
