化工社化工社 化学情報印刷レポート · 研究参考用
1,3-Diacetylbenzene → alpha1,alpha3-Dimethyl-1,3-benzenedimethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,3-Diacetylbenzene | HCID 23229 | — |
| 反応物 | Sodium borohydride | HCID 4311764 | — |
| 生成物 | alpha1,alpha3-Dimethyl-1,3-benzenedimethanol | HCID 15148377 | — |
反応手順
This mixture of stereoisomers was prepared from 1,3-diacetylbenzene by reduction with sodium borohydride as described above for the para stereoisomers. The mixture of stereoisomers was isolated as a semisolid. It appeared as a single spot on TLC and as a single peak on VPC.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05166062 |
| 出典データセット | uspto-grants-1992_11 |
| ORD ID | ord-546ecb5962634cd395c40460dcb9740d |
| 出典メモ | uspto-grants-1992_11 |