化工社化工社 化学情報印刷レポート · 研究参考用
4-Hydroxybutanal → 1,4-Butanediol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Hydroxybutanal | HCID 93093 | — |
| 反応物 | 3-Hydroxy-2-methylpropanal | HCID 11029762 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 1,4-Butanediol | HCID 8064 | — |
| 生成物 | Methylpropanediol | HCID 75103 | — |
反応手順
The invention relates to the preparation of tetrahydrofuran. In particular, a mixture of 4-hydroxybutanal and 3-hydroxy-2-methylpropanal is hydrogenated in the presence of a supported transition metal catalyst to give tetrahydrofuran as the major product, and 1,4-butanediol and 2-methyl-1,3-propanediol as minor products.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05166370 |
| 出典データセット | uspto-grants-1992_11 |
| ORD ID | ord-1f83adcc5a764fc89dcdd93799091101 |
| 出典メモ | uspto-grants-1992_11 |