化工社化工社 化学情報印刷レポート · 研究参考用
Stearic Acid → 1-Chlorooctadecane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Stearic Acid | HCID 5281 | — |
| 反応物 | Phosgene | HCID 6371 | — |
| 生成物 | 1-Chlorooctadecane | HCID 18815 | 99.9% |
反応手順
The experimental method described in Example 1 is used, and 2,746 g (10 moles) of technical grade stearic acid and the catalyst phase (342 g) obtained in Example 1 are initially taken. 1,089 g (11 moles) of gaseous phosgene are then introduced. The product phase contains 2,930 g (99.9% yield) of stearyl chloride having a purity of 97% (determined by IR spectroscopy); the iodine color number is 30.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05166427 |
| 出典データセット | uspto-grants-1992_11 |
| ORD ID | ord-036e48ed98a246a49a6fe4680c24cf33 |
| 出典メモ | uspto-grants-1992_11 |