化工社化工社 化学情報印刷レポート · 研究参考用
D-(-)-Fructose → 3-Hydroxybutyrate 4-hydroxybutyrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | D-(-)-Fructose | HCID 5984 | — |
| 反応物 | Sodium Oxybate | HCID 23663870 | — |
| 生成物 | 3-Hydroxybutyrate 4-hydroxybutyrate | HCID 86749183 | 20% |
反応手順
The procedure of Example 2 was repeated except that the fructose was replaced with sodium 4-hydroxybutyrate (manufactured by Aldrich Corporation) to produce 1.2 g of 3-hydroxybutyrate-4-hydroxybutyrate copolymer (comprising 20% by mole of 4-hydroxybutyrate unit) having a number average molecular weight of 467,000. The thus produced copolymer product was added to a 100 ml solution comprising 1 volume of aqueous solution of sodium hypochroride (manufactured by Wako Pharmaceutical K.K.) and 1 volume of distilled water, and the suspension was heated to 50° C. for 2 hours. The resulting product had a number average molecular weight of 182,000.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05480394 |
| 出典データセット | uspto-grants-1996_01 |
| ORD ID | ord-8a5039f60afa42afa6418534e0bb4e31 |
| 出典メモ | uspto-grants-1996_01 |