化工社化工社 化学情報印刷レポート · 研究参考用
2,2,2-Trifluoroethanol → Fluoroformic acid 2,2,2-trifluoroethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,2,2-Trifluoroethanol | HCID 6409 | — |
| 反応物 | Carbonyl fluoride | HCID 9623 | — |
| 生成物 | Fluoroformic acid 2,2,2-trifluoroethyl ester | HCID 14493380 | — |
反応手順
236faE (CAS Reg. No. 20193-67-3) has been prepared by reaction of 2,2,2-trifluoroethanol with carbonyl fluoride to give the intermediate, CF3CH2OCOF, which was in turn reacted with sulfur tetrafluoride at 150°-200° C. to give the product as disclosed by Eisemann in U.S. Pat. No. 3,394,878.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05480572 |
| 出典データセット | uspto-grants-1996_01 |
| ORD ID | ord-b7bbf60dbf5b45ef8b59875145d19808 |
| 出典メモ | uspto-grants-1996_01 |