関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | DL-Arabinose | HCID 854 | — |
| 反応物 | L-Lysine | HCID 5962 | — |
| 反応物 | Aldehydo-D-ribose | HCID 5311110 | — |
| 反応物 | HCID 178418600 | HCID 178418600 | — |
| 生成物 | Pentosidine | HCID 119593 | — |
反応手順
In order to confirm the pentose-derived nature of the native fluorophore 100 mM each of L-lysine, L-arginine and D-ribose were heated for 1 hour at 80° C. Injection of a small amount of this synthetic material on HPLC revealed a major fluorescent peak coeluting with the native fluorophore. (see FIG. 5) In order to substantiate the proposed structure, the synthetic fluorophore was prepared preparatively and purified. Total yield was 21 mg; i.e., 0.02% of the reactants.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05480807 |
|---|
| 出典データセット | uspto-grants-1996_01 |
|---|
| ORD ID | ord-8357ab42bf30496287c2be5cf03b34d8 |
|---|
| 出典メモ | uspto-grants-1996_01 |
|---|
