化工社化工社 化学情報印刷レポート · 研究参考用
Trifluoroacetic acid → Caprine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trifluoroacetic acid | HCID 6422 | — |
| 反応物 | tert-butyl (2S)-2-aminohexanoate | HCID 12451446 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Caprine | HCID 21236 | — |
反応手順
23.5 mg of L-N-[(2R or S)-5-ethylthio-2-(1-naphthylmethyl)pentanoyl]norleucine tert-butyl ester was dissolved in 0.2 ml of dichloromethane, and 0.1 ml of trifluoro acetic acid was added thereto. The mixture was stirred at room temperature for four hours. Then, the reaction solution was concentrated under reduced pressure to obtain 20.7 mg of L-N-[(2R or S)-5-ethylthio-2-(1-naphthylmethyl)pentanoyl]norleucine as colorless solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05481036 |
| 出典データセット | uspto-grants-1996_01 |
| ORD ID | ord-aa312e5f1bd544c6952f2a6f19a3f20f |
| 出典メモ | uspto-grants-1996_01 |