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Octylbenzene → HCID 13742410、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Octylbenzene | HCID 16607 | — |
| 反応物 | Glyoxal, phenyl-, hydrate | HCID 12215922 | — |
| 触媒 | Titanium Tetrachloride | HCID 24193 | — |
| 溶媒 | 1,1-Dichloroethane | HCID 6365 | — |
| 生成物 | HCID 13742410 | HCID 13742410 | — |
反応手順
Phenylglyoxal monohydrate (608 mg, 4 mM) and n-octylbenzene (1.77 ml, 8 mM) were dissolved in dichloroethane (8 ml), titanium tetrachloride (0.66 ml, 6 mM) was added, and reacted at room temperature for 30 minutes. Using the same procedure as in Example 1, 4'-n-octylbenzoin was obtained as crystal (810.0 mg, 62.6% yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05484689 |
| 出典データセット | uspto-grants-1996_01 |
| ORD ID | ord-7915a95a149c4f35a700216a2be8fa61 |
| 出典メモ | uspto-grants-1996_01 |