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HRID 375294作成日:2026年10月25日

3-(2,4-Dimethoxyphenyl)prop-2-enoic acid → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,4-dimethoxyphenyl)ethenyl)-, (E)-

https://huagongshe.com/reaction/375294

反応式

関与物質

役割名称HCID仕込み量
反応物3-(2,4-Dimethoxyphenyl)prop-2-enoic acidHCID 85636—
反応物5,6-Diamino-1,3-diethyluracilHCID 4572133—
生成物1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,4-dimethoxyphenyl)ethenyl)-, (E)-HCID 644885320%

反応手順

Substantially the same procedure as in Example 7 was repeated using 2.50 g (12.6 mmol) of 5,6-diamino-1,3diethyluracil and 2.89 g (13.9 mmol) of 2,4-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide/ethanol to give 0.92 g (yield 20%) of Compound 68 as yellow crystals.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05484920
出典データセットuspto-grants-1996_01
ORD IDord-5849e0e2147e4075a013afb0933396a6
出典メモuspto-grants-1996_01