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HRID 375296作成日:2026年10月24日

5,6-Diamino-1,3-diethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,5-dimethyl-4-methoxy)phenyl)ethenyl)-, (E)-

https://huagongshe.com/ja/reaction/375296

反応式

関与物質

役割名称HCID仕込み量
反応物5,6-Diamino-1,3-diethyluracilHCID 4572133—
反応物4-Methoxy-2,5-dimethylcinnamic acidHCID 5199898—
生成物1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,5-dimethyl-4-methoxy)phenyl)ethenyl)-, (E)-HCID 644885952.3%

反応手順

Substantially the same procedure as in Example 7 was repeated using 2.5 g (12.6 mmol) of 5,6-diamino-1,3-diethyluracil and 2.9 g (13.9 mmol) of 4-methoxy-2,5-dimethylcinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 2.43 g (yield 52%) of Compound 74 as white crystals.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05484920
出典データセットuspto-grants-1996_01
ORD IDord-88795606de874e8584742da57ead9c5a
出典メモuspto-grants-1996_01