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HRID 375298作成日:2026年10月26日

3-(1,3-Benzodioxol-5-yl)prop-2-enoic acid → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(1,3-benzodioxol-5-yl)ethenyl)-1,3-diethyl-, (E)-

https://huagongshe.com/reaction/375298

反応式

関与物質

役割名称HCID仕込み量
反応物3-(1,3-Benzodioxol-5-yl)prop-2-enoic acidHCID 16917—
反応物5,6-Diamino-1,3-diethyluracilHCID 4572133—
生成物1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(1,3-benzodioxol-5-yl)ethenyl)-1,3-diethyl-, (E)-HCID 644886338%

反応手順

Substantially the same procedure as in Example 7 was repeated using 2.0 g (10.1 mmol) of 5,6-diamino-1,3-diethyluracil and 2.33 g (12.1 mmol) of 3,4methylenedioxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide/water to give 1.34 g (yield 38%) of Compound 78 as a yellowish green powder.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05484920
出典データセットuspto-grants-1996_01
ORD IDord-95ac9307624d4b3bab7f5b9483857a51
出典メモuspto-grants-1996_01