化工社化工社 化学情報印刷レポート · 研究参考用
5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,3-dimethyl-4-methoxyphenyl)ethenyl)-, (E)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5,6-Diamino-1,3-dimethyluracil | HCID 79501 | — |
| 反応物 | 4-Methoxy-2,3-dimethylcinnamic acid | HCID 53401770 | — |
| 生成物 | 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,3-dimethyl-4-methoxyphenyl)ethenyl)-, (E)- | HCID 6448865 | 22% |
反応手順
Substantially the same procedure as in Example 7 was repeated using 1.74 g (10.2 mmol) of 5,6-diamino-1,3-dimethyluracil and 2.42 g (11.8 mmol) of 4-methoxy-2,3dimethylcinnamic acid. Then, the resultant crude crystals were recrystallized from acetonitrile to give 750 mg (yield 22%) of Compound 84 as a white powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05484920 |
| 出典データセット | uspto-grants-1996_01 |
| ORD ID | ord-b85bc2fbc6164ae689259bd2b7e5fedf |
| 出典メモ | uspto-grants-1996_01 |