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HRID 375303作成日:2026年10月25日

5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,3-dimethoxyphenyl)ethenyl)-1,3-dimethyl-, (E)-

https://huagongshe.com/reaction/375303

反応式

関与物質

役割名称HCID仕込み量
反応物5,6-Diamino-1,3-dimethyluracilHCID 79501—
反応物2,3-Dimethoxycinnamic acidHCID 99525—
生成物1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,3-dimethoxyphenyl)ethenyl)-1,3-dimethyl-, (E)-HCID 5379232—

反応手順

Substantially the same procedure as in Example 7 was repeated using 2.50 g (14.7 mmol) of 5,6-diamino-1,3-dimethyluracil and 3.37 g (16.2 mmol) of 2,3-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from ethanol/water to give 1.03 g (yield of Compound 88 as pale yellow needles.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05484920
出典データセットuspto-grants-1996_01
ORD IDord-d7408d53891749b8975fc090d0999035
出典メモuspto-grants-1996_01