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HRID 375304作成日:2026年10月26日

5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,4-dimethoxyphenyl)ethenyl)-1,3-dimethyl-, (E)-

https://huagongshe.com/reaction/375304

反応式

関与物質

役割名称HCID仕込み量
反応物5,6-Diamino-1,3-dimethyluracilHCID 79501—
反応物3-(2,4-Dimethoxyphenyl)prop-2-enoic acidHCID 85636—
生成物1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,4-dimethoxyphenyl)ethenyl)-1,3-dimethyl-, (E)-HCID 644886811%

反応手順

Substantially the same procedure as in Example 7 was repeated using 1.0 g (5.88 mmol) of 5,6-diamino-1,3-dimethyluracil and 1.35 g (6.48 mmol) of 2,4-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide to give 221 mg (yield 11%) of Compound 90 as pale yellow grains.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05484920
出典データセットuspto-grants-1996_01
ORD IDord-4f385ec37bbe45b6b8760ea462141072
出典メモuspto-grants-1996_01