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HRID 375310作成日:2026年10月25日

3-(p-Tolyl)acrylic acid → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(4-methylphenyl)ethenyl)-, (E)-

https://huagongshe.com/reaction/375310

反応式

関与物質

役割名称HCID仕込み量
反応物3-(p-Tolyl)acrylic acidHCID 15835—
反応物5,6-Diamino-1,3-diethyluracilHCID 4572133—
生成物1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(4-methylphenyl)ethenyl)-, (E)-HCID 644888254%

反応手順

Substantially the same procedure as in Example 7 was repeated using 3.00 g (15.1 mmol) of 5,6-diamino-1,3-diethyluracil and 2.70 g (16.7 mmol) of 4-methylcinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane to give 2.64 g (yield 54%) of Compound 106 as pale yellow needles.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05484920
出典データセットuspto-grants-1996_01
ORD IDord-d15e897f5f674bd9997aef04cadf68a9
出典メモuspto-grants-1996_01