化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 3-(3-Fluorophenyl)propanoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 3-(3-Fluorophenyl)propionic acid | HCID 2737489 | — |
| 生成物 | 3-(3-Fluorophenyl)propanoyl chloride | HCID 18993501 | — |
反応手順
A solution of 3-fluorohydrocinnamic acid (28 g) in thionyl chloride (90 ml) was heated at reflux for 3 hours. 3-Fluorohydrocinnamoyl chloride (27 g) was isolated by distillation (150°-110° C. @ ca 20 mm.Hg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05486541 |
| 出典データセット | uspto-grants-1996_01 |
| ORD ID | ord-66e7a4465c454ece8d230e1ae0a91cbd |
| 出典メモ | uspto-grants-1996_01 |