化工社化工社 化学情報印刷レポート · 研究参考用
Diethylamine → Benzoic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethylamine | HCID 8021 | — |
| 反応物 | 2-Chloro-5-(fluorosulpho)benzoic acid | HCID 88873 | — |
| 溶媒 | 1,2-Dichloroethane | HCID 11 | — |
| 生成物 | Benzoic Acid | HCID 243 | — |
反応手順
A mixture of 2-chloro-5-(fluorosulfonyl)benzoic acid (11.93 g, 0.05 mol), diethylamine (10.97 g, 0.15 mol) and 1,2-dichloroethane (100 mL) was refluxed for 8 hours. The reaction mixture was evaporated and the residue was dissolved in ethyl acetate. A solid was collected by filtration and the filtrate was evaporated to dryness to afford 15.5 g of 2-chloro-5-diethylaminosulfonyl)benzoic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05488055 |
| 出典データセット | uspto-grants-1996_01 |
| ORD ID | ord-498b6d423ed8427fba6d206335405625 |
| 出典メモ | uspto-grants-1996_01 |