ホームMCPワークベンチSkills
ホームワークベンチ通知マイページ
llms.txt · MCPガイドプライバシーポリシー · 利用規約 · サポートv1.8.0
  1. ホーム
  2. /反応

Cesium carbonate → HCID 18991734、化合物

HRID 376061
ノート
印刷プレビュー

反応式

HRID 376061 の反応式
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]([N:10]([CH:14]([CH3:16])[CH3:15])[CH:11]([CH3:13])[CH3:12])=[O:9])=[CH:4][C:3]=1[O:17][CH3:18].C(=O)([O-])[O-].[Cs+].[Cs+].Br[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][O:31][C:32]1[CH:37]=[CH:36][C:35]([C:38](=[NH:42])[O:39][CH2:40][CH3:41])=[CH:34][CH:33]=1>CN(C)C=O>[CH3:18][O:17][C:3]1[CH:4]=[C:5]([C:8]([N:10]([CH:11]([CH3:12])[CH3:13])[CH:14]([CH3:16])[CH3:15])=[O:9])[CH:6]=[CH:7][C:2]=1[O:1][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][O:31][C:32]1[CH:33]=[CH:34][C:35]([C:38](=[NH:42])[O:39][CH2:40][CH3:41])=[CH:36][CH:37]=1
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

5

反応物 3

HCID 10796Cesium carbonateHCID 18991675HCID 18991675、化合物HCID 217472594-Hydroxy-3-methoxy-N,N-di(propan-2-yl)benzamide

生成物 1

HCID 18991734HCID 18991734、化合物

試薬・触媒・溶媒 1

HCID 6228Dimethylformamide溶媒

反応条件

温度
70 °C

実験手順

A stirred solution of 4-hydroxy-3-methoxy-N,N-bis(1-methylethyl)benzenecarboxamide (319 mg, 1.27 mmol) in 3.5 mL anhydrous N,N-dimethylformamide is treated with cesium carbonate (435 mg, 1.33 mmol) and ethyl 4-[5-bromopentoxy]benzenecarboximidoate (400 mg, 1.27 mmol) and heated at 70° C. for 1.0 hours. After cooling to room temperature, the reaction is partitioned between ethyl acetate and water and the organics washed with brine, dried over sodium sulfate and concentrated in vacuo to afford a yellow oil. This material is purified by chromatography on silica gel (22 g) with 30-75% ethyl acetate/hexanes as the eluent to afford ethyl 4-[5-[2-methoxy-4-[N,N-bis(1-methylethyl)aminocarbonyl]phenoxy]pentoxy]benzenecarboximidoate as a colorless oil.

後処理

  1. temperatureAfter cooling to room temperature
  2. customthe reaction is partitioned between ethyl acetate and water
  3. washthe organics washed with brine
  4. dry with materialdried over sodium sulfate
  5. concentrationconcentrated in vacuo
  6. customto afford a yellow oil
  7. customThis material is purified by chromatography on silica gel (22 g) with 30-75% ethyl acetate/hexanes as the eluent

出典と根拠

ORDレコード
ord-bba568bde14a4a99bea20e7060532139
出典データセット
uspto-grants-1996_01
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US05488160

反応ノート

読み込み中…

このページの内容参加物反応条件実験手順後処理出典と根拠反応ノート