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1,3-Dioxane, 2-(2-bromoethyl)- → N-[2-(1,3-dioxane-2-yl)ethyl]-4-(4-methylstyryl)-quinolinium bromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,3-Dioxane, 2-(2-bromoethyl)- | HCID 520656 | — |
| 反応物 | 4-(4-Methylstyryl)quinoline | HCID 54172084 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | N-[2-(1,3-dioxane-2-yl)ethyl]-4-(4-methylstyryl)-quinolinium bromide | HCID 70262692 | 70% |
反応手順
4-(4-methylstyryl)quinoline (0.245 g) and 2-(2-bromoethyl) 1,3-dioxane (0.195 g) were mixed and refluxed in ethylacetate (1.5 ml) for 18 hours. Yellow-green precipitate was separated by filtration, washed with ethyl ether and dried in vacuo to give 0.308 g of N-[2-(1,3-dioxane-2-yl)ethyl]-4-(4-methylstyryl)-quinolinium bromide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06020436 |
| 出典データセット | uspto-grants-2000_02 |
| ORD ID | ord-4d646bf149474aefa20541ab75a3405f |
| 出典メモ | uspto-grants-2000_02 |