関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 2-Methoxy-1-phenylethanone | HCID 77698 | — |
| 反応物 | 4-Azidobenzaldehyde | HCID 90385 | — |
| 生成物 | 3-(4-Azidophenyl)-1-(2-methoxyphenyl)prop-2-en-1-one | HCID 54148794 | — |
反応手順
In a 500-ml flask were placed 15 g of 2-methoxyacetophenone (made by Aldrich Co., 99% purity), 15 g of p-azidobenzaldehyde (manufactured by Kanto Chemical Co., Ltd.), 50 g of 10% aqueous solution of NaOH, and 50 g of methanol. The mixture was stirred in a yellow light at 25° C. for 24 hours. After completion of the reaction, the deposited crystals were filtered, washed with water, dried, and recrystallized from ethanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04722883 |
|---|
| 出典データセット | uspto-grants-1988_02 |
|---|
| ORD ID | ord-844bfa4964764092a84084123ac463f1 |
|---|
| 出典メモ | uspto-grants-1988_02 |
|---|
