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3-Pyrrolidone, 1-methyl- → 3-(3-Methyl-5-isoxazolyl)methylene-1-methylpiperidine oxalate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Pyrrolidone, 1-methyl- | HCID 144283 | — |
| 反応物 | Isoxazole, 3-methyl-5-[(trimethylsilyl)methyl]- | HCID 10986681 | — |
| 反応物 | HCID 70087037 | HCID 70087037 | — |
| 生成物 | 3-(3-Methyl-5-isoxazolyl)methylene-1-methylpiperidine oxalate | HCID 70249731 | — |
反応手順
3-(3-methyl-5-isoxazolyl)methylene-1-methylpyrolidine oxalate, compound 8, and (E) 3-(3-methyl-5-isoxazolyl)methylene-1-methylpyrrolidine oxalate, compound 9, starting form 1-methyl-pyrrolidin-3-one (J. Amer. Chem. Soc., 55, 1933, 1233-1241) and 3-methyl-5-trimethylsilylmethyl-isoxazole.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06022868 |
| 出典データセット | uspto-grants-2000_02 |
| ORD ID | ord-48109cd8a4e949bdb140a50f345e55d4 |
| 出典メモ | uspto-grants-2000_02 |