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Perfluorooctyl iodide → 2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundec-2-enyloxy)ethyl hydrogen sulfate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Perfluorooctyl iodide | HCID 10491 | — |
| 反応物 | Allyloxyethyl sulfate | HCID 20611889 | — |
| 生成物 | 2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoroundec-2-enyloxy)ethyl hydrogen sulfate | HCID 131730836 | — |
反応手順
Crystalline allyloxyethyl sulfate (Na salt) from the preparation shown in example 2 was perfluoroalkylated using the procedure of example 7 and C8F17I to produce 2-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundec-2-enyloxy)ethyl hydrogen sulfate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08524104B1 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-9ce66c0ac6a9497f90fd9e34b54bd9d0 |
| 出典メモ | uspto-grants-2013_09 |