化工社化工社 化学情報印刷レポート · 研究参考用
Acrylic Acid → Prop-2-enoic acid--prop-2-enal (1/1)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acrylic Acid | HCID 6581 | — |
| 反応物 | Acrolein | HCID 7847 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Prop-2-enoic acid--prop-2-enal (1/1) | HCID 3084492 | — |
反応手順
Control drug: (acrylic acid:acrolein (mol)=95:5): 3.25 g freshly distilled acrolein and 79.27 g freshly distilled acrylic acid were added into a three-port flask with 520 ml absolute methanol, purged with nitrogen, 4.74 g benzoyl peroxide was added, and the solution was stirred and heated to reflux under nitrogen for 50 h. The reaction solution became a yellowish viscous liquid, which was dried under vacuum at 50-100° C. for 24 hours to form poly (acrolein-acrylic acid) named A3.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08524216B2 |
| 出典データセット | uspto-grants-2013_09 |
| ORD ID | ord-5a15d92a442f4a9a8f8753420daea0f0 |
| 出典メモ | uspto-grants-2013_09 |