戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 37735作成日:2026年10月25日

Acrylic Acid → Prop-2-enoic acid--prop-2-enal (1/1)

https://huagongshe.com/reaction/37735

反応式

関与物質

役割名称HCID仕込み量
反応物Acrylic AcidHCID 6581—
反応物AcroleinHCID 7847—
溶媒MethanolHCID 887—
生成物Prop-2-enoic acid--prop-2-enal (1/1)HCID 3084492—

反応手順

Control drug: (acrylic acid:acrolein (mol)=95:5): 3.25 g freshly distilled acrolein and 79.27 g freshly distilled acrylic acid were added into a three-port flask with 520 ml absolute methanol, purged with nitrogen, 4.74 g benzoyl peroxide was added, and the solution was stirred and heated to reflux under nitrogen for 50 h. The reaction solution became a yellowish viscous liquid, which was dried under vacuum at 50-100° C. for 24 hours to form poly (acrolein-acrylic acid) named A3.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08524216B2
出典データセットuspto-grants-2013_09
ORD IDord-5a15d92a442f4a9a8f8753420daea0f0
出典メモuspto-grants-2013_09