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HRID 37736作成日:2026年10月25日

Acrylic Acid → Prop-2-enoic acid--prop-2-enal (1/1)

https://huagongshe.com/reaction/37736

反応式

関与物質

役割名称HCID仕込み量
反応物Acrylic AcidHCID 6581—
反応物AcroleinHCID 7847—
溶媒MethanolHCID 887—
生成物Prop-2-enoic acid--prop-2-enal (1/1)HCID 3084492—

反応手順

Control drug: (acrylic acid:acrolein (mol)=90:10): 7.04 g freshly distilled acrolein and 81.43 g freshly distilled acrylic acid were added into a three-port flask with 530 ml absolute methanol, purged with nitrogen, 5.47 g benzoyl peroxide was added, and the solution was stirred and heated to reflux under nitrogen for 50 h. The reaction solution became a yellowish viscous liquid, which was dried under vacuum at 50-100° C. for 24 hours to form poly (acrolein-acrylic acid) named A5.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08524216B2
出典データセットuspto-grants-2013_09
ORD IDord-6f1d96f9b6954f10a11099f21711a51e
出典メモuspto-grants-2013_09