化工社化工社 化学情報印刷レポート · 研究参考用
2,3,4-Trichlorobenzenesulfonyl chloride → 2,3,4-Trichloro-N-(4-bromo-3-methyl-5-isoxazolyl)benzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3,4-Trichlorobenzenesulfonyl chloride | HCID 36904 | — |
| 反応物 | 4-Bromo-3-methylisoxazol-5-amine | HCID 10487519 | — |
| 生成物 | 2,3,4-Trichloro-N-(4-bromo-3-methyl-5-isoxazolyl)benzenesulfonamide | HCID 18617341 | 66% |
反応手順
2,3,4-Trichloro-N-(4-bromo-3-methyl-5-isoxazolyl)benzenesulfonamide was prepared from 5-amino-4-bromo-3-methylisoxazole and 2,3,4-trichlorobenzenesulfonyl chloride according to the procedures described in Example 30. The crude product was purified by recrystallization from ethyl acetate/hexanes to give a crystalline solid, m.p.110-113° C., yield 66%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06030991 |
| 出典データセット | uspto-grants-2000_02 |
| ORD ID | ord-eec456e3df094707b35d9f870e4964ab |
| 出典メモ | uspto-grants-2000_02 |