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Methyl iodide → 4-(3-Acetylphenyl)amino-2-amino-1,6-dimethylpyrimidinium iodide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl iodide | HCID 6328 | — |
| 反応物 | Cni H1594 | HCID 133110 | — |
| 反応物 | 2-Amino-4-(3-acetylphenyl)amino-1,6-dimethylpyrimidinium iodide | HCID 463011 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | 4-(3-Acetylphenyl)amino-2-amino-1,6-dimethylpyrimidinium iodide | HCID 12093259 | — |
反応手順
Compound No. 14 (CNI-H1494): 4-(3-acetylphenyl)amino-2-amino-6-methylpyrimidine, Compound No. 15, (0.968 g) was suspended in acetone (5 mL) containing methyl iodide (2 mL) was heated at reflux for 48 hr. Filtration after cooling gave 0.657 g of 4-(3-acetylphenyl)amino-2-amino-1,6-dimethylpyrimidinium iodide as a white powder, mp 238-40° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06297253B1 |
| 出典データセット | uspto-grants-2001_10 |
| ORD ID | ord-101f3ab2589e4a1f8d011161acc156cc |
| 出典メモ | uspto-grants-2001_10 |