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Hydrate lead acetate → Lead diacetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrate lead acetate | HCID 86584228 | — |
| 溶媒 | 2-Butoxyethanol | HCID 8133 | — |
| 生成物 | Lead diacetate | HCID 9317 | — |
反応手順
The hydrate lead acetate is dissolved in butoxyethanol (BuEtOH) (1) at 60° C. The resulting solution is kept at this temperature for two hours, and is cooled down slowly (2) to thereby form a precipitate of dehydrated lead acetate. The precipitation yield can be promoted by further cooling down the vessel containing said solution in an ice bath.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06300144B1 |
| 出典データセット | uspto-grants-2001_10 |
| ORD ID | ord-d2912ed95edd4b108b23c3a7feb1bdf4 |
| 出典メモ | uspto-grants-2001_10 |