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4-Hydroxybenzenesulfonic acid → Sodium (3-methylbutoxy)benzenesulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Hydroxybenzenesulfonic acid | HCID 4765 | — |
| 反応物 | 1-Iodo-3-methylbutane | HCID 10924 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 溶媒 | Water | HCID 962 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | Sodium (3-methylbutoxy)benzenesulfonate | HCID 131722889 | — |
反応手順
A solution of 4hydroxybenzenesulfonic acid (10.0 grams, 43.1 mmole) and sodium hydroxide (3.3 grams, 83 mmole) in water (40 mL) was mixed with a solution of 1-iodo-3methylbutane (11.3 mL, 86.4 mmole) in isopropanol (60 mL) and the resulting mixture was heated at reflux for 2 days. The isopropanol was removed by evaporation under vaccuum. The titled compound, 10.0 grams (87%), was collected by filtration washing with isopropanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06303636B1 |
| 出典データセット | uspto-grants-2001_10 |
| ORD ID | ord-148906a74d08481191dd671d2b696e2d |
| 出典メモ | uspto-grants-2001_10 |