化工社化工社 化学情報印刷レポート · 研究参考用
1-Chloro-2,4-Dinitrobenzene → 2-(2,4-Dinitrophenoxy)ethanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Chloro-2,4-Dinitrobenzene | HCID 6 | — |
| 反応物 | Ethylene Glycol | HCID 174 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | 2-(2,4-Dinitrophenoxy)ethanol | HCID 76070 | 74.5% |
反応手順
20.25 g (0.1 mole) of 2,4-dinitrochlorobenzene, 124 g (2 moles) of ethylene glycol, 82.93 g (0.6 mole) of potassium carbonate, and 600 ml of xylene were placed in a reaction vessel to be stirred by heating for 12 hours. The reacted solution was isolated by filtration, and the filtrate was concentrated. 17.0 g of 2-(2,4-dinitrophenoxy) ethanol was yielded by column purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06303742B1 |
| 出典データセット | uspto-grants-2001_10 |
| ORD ID | ord-62be93d1b7c1453a9a1721b3f0fd489f |
| 出典メモ | uspto-grants-2001_10 |