化工社化工社 化学情報印刷レポート · 研究参考用
Salicylic Acid → Sodium Salicylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Salicylic Acid | HCID 338 | — |
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Sodium | HCID 5360545 | — |
| 触媒 | Silver Nitrate | HCID 24470 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Sodium Salicylate | HCID 16760658 | — |
反応手順
An aqueous solution of sodium salicylate was prepared by adding 43.2 g of 2N sodium hydroxide to 12 g of salicylic acid in 240 g of demineralized water. This aqueous solution was simultaneously added with 120 mL of a 0.588 M aqueous solution of silver nitrate over a period of 10 s to 280 mL of a stirred aqueous solution containing 160 mL of a 5% aqueous solution of GAFAC ™ RM710 (an alkylphenyl- polyethene oxide-phosphate from GENERAL ANILINE), 80 mL of a 2% aqueous solution of NATRASOL™ 250L (a hydroxyethylcellulose from AQUALON) and 40 mL of demineralized water. 160 mL of a 5% aqueous solution of PIGMENTVERTEILER™ N (a sodium salt of polyacrylic acid from BASF) was then added to the resulting dispersion.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06306571B1 |
| 出典データセット | uspto-grants-2001_10 |
| ORD ID | ord-e866e6c6de4241159a6af5765b3c56a4 |
| 出典メモ | uspto-grants-2001_10 |