化工社化工社 化学情報印刷レポート · 研究参考用
1-Tetralone → 1,2-Dihydro-4-methylnaphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Tetralone | HCID 10724 | — |
| 反応物 | HCID 178418373 | HCID 178418373 | — |
| 生成物 | 1,2-Dihydro-4-methylnaphthalene | HCID 582327 | 68% |
反応手順
α-Tetralone was reacted with methylmagnesium iodide as described in J. Org. Chem., 26, 4165 (1961), without isolation of the intermediate 1-methyl-1-tetralol, to give the desired product, after distillation, in 68% yield as a colorless oil, boiling point 55-57° C. at 0.8 mm Hg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06307085B1 |
| 出典データセット | uspto-grants-2001_10 |
| ORD ID | ord-f467ee58ecf64abf885a0a6430418e94 |
| 出典メモ | uspto-grants-2001_10 |