Ethylene di(S-thioacetate) → GDMA Methacrylic Acid

反応式

[CH2:1]([O:8][C:9]([CH2:11][SH:12])=[O:10])[CH2:2][O:3][C:4]([CH2:6][SH:7])=[O:5].C1CCC(O)([C:19]([C:21]2[CH:26]=CC=C[CH:22]=2)=[O:20])CC1>>[CH2:2]([O:3][C:4]([CH2:6][SH:7])=[O:5])[CH2:1][O:8][C:9]([CH2:11][SH:12])=[O:10].[C:19]([OH:3])(=[O:20])[C:21]([CH3:26])=[CH2:22]

参加物

反応物 2

HCID 61059Ethylene di(S-thioacetate)

HCID 703551-Hydroxycyclohexyl phenyl ketone

生成物 1

HCID 131721771GDMA Methacrylic Acid

実験手順

GDMA (556.8 g, 5.15 eq.) was weighed into a 2000 ml, three neck, round bottom flask. MAA (442.9 g, 5.15 eq.) and Irgacure 184 (1.5 g) were weighed into a 500 ml addition funnel equipped with a Teflon stop cock.

出典と根拠

ORDレコード: ord-e7bb9e62c4d24caa9cf852baa657d138
出典データセット: uspto-grants-2001_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06310161B1

反応ノート

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