化工社化工社 化学情報印刷レポート · 研究参考用
Cyclohexyl isocyanate → HCID 178418497、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexyl isocyanate | HCID 18502 | — |
| 反応物 | 3-[4-(4-Chlorophenethyl)piperazin-1-yl]propanethiol | HCID 13731125 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | HCID 178418497 | HCID 178418497 | 170.7% |
反応手順
The procedure described in Example 35 was followed, using 1.7 g of cyclohexyl isocyanate, 4.0 g of 3-[4-(4-chlorophenethyl)piperazin-1-yl]propanethiol and 100 ml of methylene chloride, to give 3.8 g (58% of theory) of N-cyclohexyl-S-{3-[4-(4-chlorophenethyl)piperazin-1-yl]propyl}thiocarbamate dihydrochloride as a white crystalline solid, M.p. 262°-267° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04722926 |
| 出典データセット | uspto-grants-1988_02 |
| ORD ID | ord-a34cebc025d14918a8b53e7fb7577a4a |
| 出典メモ | uspto-grants-1988_02 |