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1-Isocyanato-4-methoxybenzene → HCID 178418524、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Isocyanato-4-methoxybenzene | HCID 79443 | — |
| 反応物 | 3-{4-[3-(4-Chlorophenyl)propyl]piperazin-1-yl}propanethiol | HCID 13731129 | — |
| 溶媒 | Methyl, chloro- | HCID 5378701 | — |
| 生成物 | HCID 178418524 | HCID 178418524 | 146.1% |
反応手順
The procedure described in Example 35 was followed, using 2.0 g of 4-methoxyphenyl isocyanate, 4.0 g of 3-{4-[3-(4-chlorophenyl)propyl]piperazin-1-yl}propanethiol and 100 ml of methylene chlorine to give 3.4 g (48% of theory) of N-(4-methoxyphenyl)-S-{3-[4-[3-(4-chlorophenyl)propyl]piperazin-1-yl]propyl}thiocarbamate dihydrochloride hemihydrate as a white crystalline solid, M.p. 240°-244° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04722926 |
| 出典データセット | uspto-grants-1988_02 |
| ORD ID | ord-0346a80a37094debaa473c96709fc5a5 |
| 出典メモ | uspto-grants-1988_02 |