Isopropanol → Rac-[1-(4-chloro-phenyl)-2-(4-isopropoxy-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester
反応式
[C:1]([O:5][C:6](=[O:25])[NH:7][CH:8]([C:18]1[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][CH:19]=1)[C:9]([C:11]1[CH:16]=[CH:15][C:14]([OH:17])=[CH:13][CH:12]=1)=[O:10])([CH3:4])([CH3:3])[CH3:2].[CH:26](O)([CH3:28])[CH3:27]>>[C:1]([O:5][C:6](=[O:25])[NH:7][CH:8]([C:18]1[CH:19]=[CH:20][C:21]([Cl:24])=[CH:22][CH:23]=1)[C:9]([C:11]1[CH:16]=[CH:15][C:14]([O:17][CH:26]([CH3:28])[CH3:27])=[CH:13][CH:12]=1)=[O:10])([CH3:4])([CH3:2])[CH3:3]参加物
3
実験手順
The title compound was prepared from rac-[1-(4-chloro-phenyl)-2-(4-hydroxy-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester and isopropanol in analogy to Example 9c): MS (ISP): 404.4 (M+H)+.
出典と根拠
- ORDレコード
- ord-594a3da269344c3fbd750182cc07ce2a
- 出典データセット
- uspto-grants-2013_02
- 特許番号
- US08367838B2
反応ノート
読み込み中…