化工社化工社 化学情報印刷レポート · 研究参考用
4-Bromodiphenyl Ether → Rac-[1-(3,4-dichloro-phenyl)-2-oxo-2-(4-phenoxy-phenyl)-ethyl]-carbamic acid tert-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Bromodiphenyl Ether | HCID 7565 | — |
| 反応物 | Rac-[(3,4-dichloro-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester | HCID 87442373 | — |
| 生成物 | Rac-[1-(3,4-dichloro-phenyl)-2-oxo-2-(4-phenoxy-phenyl)-ethyl]-carbamic acid tert-butyl ester | HCID 68408309 | — |
反応手順
The title compound was prepared from rac-[(3,4-dichloro-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester (Intermediate 9) and 1-bromo-4-phenoxy-benzene in analogy to Example 1a): MS (ISP): 472.0 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08367838B2 |
| 出典データセット | uspto-grants-2013_02 |
| ORD ID | ord-76d7d4654522401ca7e418f93e3fc780 |
| 出典メモ | uspto-grants-2013_02 |