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Rac-[(4-chloro-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester → Rac-[1-(4-chloro-phenyl)-2-[2-fluoro-4-(2,2,3,3,3-pentafluoro-propoxy)-phenyl]-2-oxo-ethyl]-carbamic acid tert-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Rac-[(4-chloro-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester | HCID 71663866 | — |
| 反応物 | 1-Bromo-2-fluoro-4-(2,2,3,3,3-pentafluoro-propoxy)-benzene | HCID 87443298 | — |
| 生成物 | Rac-[1-(4-chloro-phenyl)-2-[2-fluoro-4-(2,2,3,3,3-pentafluoro-propoxy)-phenyl]-2-oxo-ethyl]-carbamic acid tert-butyl ester | HCID 87443451 | — |
反応手順
The title compound was prepared from rac-[(4-chloro-phenyl)-(methoxy-methyl-carbamoyl)-methyl]-carbamic acid tert-butyl ester (Intermediate 8) and 1-bromo-2-fluoro-4-(2,2,3,3,3-pentafluoro-propoxy)-benzene (Intermediate 34) in analogy to Example 1a): MS (ISN): 510.3 (M−H)−.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08367838B2 |
| 出典データセット | uspto-grants-2013_02 |
| ORD ID | ord-01e7387d733e4c04b6fbc4cae614dfb6 |
| 出典メモ | uspto-grants-2013_02 |