化工社化工社 化学情報印刷レポート · 研究参考用
3-Isopropoxybenzeneboronic acid → Rac-[1-(3,4-dichloro-phenyl)-2-(3'-isopropoxy-biphenyl-4-yl)-2-oxo-ethyl]-carbamic acid tert-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Isopropoxybenzeneboronic acid | HCID 5083932 | — |
| 反応物 | Rac-[1-(3,4-dichloro-phenyl)-2-(4-iodo-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester | HCID 68409915 | — |
| 生成物 | Rac-[1-(3,4-dichloro-phenyl)-2-(3'-isopropoxy-biphenyl-4-yl)-2-oxo-ethyl]-carbamic acid tert-butyl ester | HCID 68408675 | — |
反応手順
The title compound was prepared from rac-[1-(3,4-dichloro-phenyl)-2-(4-iodo-phenyl)-2-oxo-ethyl]-carbamic acid tert-butyl ester and 3-isopropoxyphenylboronic acid in analogy to Example 2b): MS (ISN): 512.3 and 514.3 (M−H)−.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08367838B2 |
| 出典データセット | uspto-grants-2013_02 |
| ORD ID | ord-fc555b2ce66d455582447e23789f4dd5 |
| 出典メモ | uspto-grants-2013_02 |