HCID 19017302、化合物 → Ethyl 4-bromobenzene-1-carboximidate

HRID 385750

反応式

HRID 385750 の反応式
Cl.[Br:2][C:3]1[CH:13]=[CH:12][C:6]([C:7](=[NH:11])[O:8][CH2:9][CH3:10])=[CH:5][CH:4]=1>CCO>[Br:2][C:3]1[CH:4]=[CH:5][C:6]([C:7](=[NH:11])[O:8][CH2:9][CH3:10])=[CH:12][CH:13]=1

参加物

3

反応物 1

HCID 19017302HCID 19017302、化合物

生成物 1

HCID 10466301Ethyl 4-bromobenzene-1-carboximidate

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

Into a 3000 mL 3-necked flask was placed EtOH (2000 mL). To this was added sequentially Na (7.13 g, 310 mmol) and ethyl 4-bromobenzimidate hydrochloride (82 g, 310 mmol). The resulting solution was allowed to stir for two hours at room temperature, and filtered. The filtrate was evaporated to afford ethyl 4-bromobenzenecarboximidoate as a white solid.

後処理

  1. customInto a 3000 mL 3-necked flask was placed
  2. filtrationfiltered
  3. customThe filtrate was evaporated

出典と根拠

ORDレコード
ord-1e485ae0b4044980a5196007bf263f41
出典データセット
uspto-grants-2013_02
特許番号
US08367706B2

関連ノート

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