関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 3-Bromo-4-methoxyphenylacetic acid | HCID 136615 | — |
| 触媒 | Hydrochloric Acid | HCID 313 | — |
| 生成物 | Ethyl 3-bromo-4-methoxyphenylacetate | HCID 57419861 | — |
反応手順
3-Bromo-4-methoxyphenylacetic acid (4.1 g, 16.7 mmol) in EtOH (100 mL) was treated with concentrated HCl (2 drops) and heated to 80° C. for 3 days. After cooling to room temperature, the mixture was concentrated to give the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08524748B2 |
|---|
| 出典データセット | uspto-grants-2013_09 |
|---|
| ORD ID | ord-030b5dbf3810429cbd2c12d01eaaf0e3 |
|---|
| 出典メモ | uspto-grants-2013_09 |
|---|
