化工社化工社 化学情報印刷レポート · 研究参考用
Hydroxylamine → (E)-4-bromo-1-naphthaldehyde oxime
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydroxylamine | HCID 787 | — |
| 反応物 | 4-Bromo-1-naphthaldehyde | HCID 4640413 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | (E)-4-bromo-1-naphthaldehyde oxime | HCID 74016047 | — |
反応手順
Hydroxylamine (50% aqueous, 0.37 ml) is added to a solution of 4-bromo-naphthalene-1-carbaldehyde (0.7 g) in methanol (6 ml). After 16 hours at room temperature the reaction is concentrated in vacuo to yield crude 4-bromo-naphthalene-1-carbaldehyde oxime, which is used in the next step without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08377942B2 |
| 出典データセット | uspto-grants-2013_02 |
| ORD ID | ord-2e7b1da0e29743ba91047d2ec95dec3e |
| 出典メモ | uspto-grants-2013_02 |