化工社化工社 化学情報印刷レポート · 研究参考用
Isobutyric Acid → Tetramethylammonium Isobutyrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isobutyric Acid | HCID 6590 | — |
| 反応物 | Tetramethylammonium hydroxide | HCID 60966 | — |
| 生成物 | Tetramethylammonium Isobutyrate | HCID 21900158 | — |
反応手順
To a 20 L, round bottom flask was added isobutyric acid (1300 mL, 14 mol), and an aqueous solution of 25% tetramethylammonium hydroxide (5 L, 14 mol). The water was removed under reduced pressure, and azeotroped with toluene (2×2 L) to leave the product (4b) as an amber liquid, which was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08377956B2 |
| 出典データセット | uspto-grants-2013_02 |
| ORD ID | ord-4b1807cfca2845acbb98fb1b7efb445c |
| 出典メモ | uspto-grants-2013_02 |