化工社化工社 化学情報印刷レポート · 研究参考用
Nitric Acid → 2,4-Dimethyl-5-nitroaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Nitric Acid | HCID 944 | — |
| 反応物 | 2,4-Dimethylaniline | HCID 7250 | — |
| 溶媒 | Sulfuric Acid | HCID 1118 | — |
| 生成物 | 2,4-Dimethyl-5-nitroaniline | HCID 228007 | — |
反応手順
To a mixture of 2,4-dimethylaniline (10 mmol) in 5 mL of conc. H2SO4, fuming HNO3 (90%; 0.6 mL) was added dropwise at 0° C. The resulting mixture was stirred for 12 h at RT and then slowly poured into ice. The solid was collected by filtration and dried to yield 2,4-dimethyl-5-nitroaniline as a yellow solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08377983B2 |
| 出典データセット | uspto-grants-2013_02 |
| ORD ID | ord-38f61b6dd6a747a09f3247a5f0ece124 |
| 出典メモ | uspto-grants-2013_02 |